Synthesis of 1-α- methylallylthiocarb-14C-amoyl-2-methylthiocarbamoylhydrazine
✍ Scribed by V. J. Feil; P. W. Aschbacher; C. H. Lamoureux
- Book ID
- 102374922
- Publisher
- John Wiley and Sons
- Year
- 1970
- Tongue
- French
- Weight
- 108 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0022-2135
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📜 SIMILAR VOLUMES
## Abstract 4‐|2‐(Dimethylamino)ethyl‐2‐^14^C| phenol (hordenine‐α‐^14^C) has been synthesised in three steps from |^14^C|potassium cyanide and __p__‐benzyloxybenzyl chloride which in turn was obtained in four steps from __p__‐hydroxybenzoic acid.
## Abstract [1‐^14^C]‐2,2‐Difluoroethene was synthesized from [^14^C]‐formaldehyde using a modification of the Wadsworth‐Emmons reaction, __via__ formation of the intermediate (EtO)~2~P(O)CF~2~^14^CH~2~OSiMe~3~. This highly volatile product was collected in a liquid nitrogen trap at a purity of >97