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Synthesis, crystal structure and characterization of new tetranuclear Ag(I) complex with 5-aminoisophthalate

✍ Scribed by Xiao-Wu Lei; Fang-Xia Zhou; Ming-Feng Wang; Hui-Ping Zhang; Cheng-Yang Yue; Mao-Chun Hong

Book ID
118460448
Publisher
Elsevier Science
Year
2013
Tongue
English
Weight
699 KB
Volume
27
Category
Article
ISSN
1387-7003

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The reaction of 4-amino-6-methyl-1,2,4-triazine-3(2 H)-thione-5-one (AMTTO) with silver(I) nitrate in methanol gives the complex [Ag(AMTTO) 2 ]NO 3 (1). 1 was characterized by IR and 13 C NMR spectroscopy and by an X-ray structure analysis [space group C2/c, Z = 4, lattice dimensions at Β±80 Β°C: a =