Synthesis and X-ray crystal structure of 3-deoxy-3-fluoro-β-D-allopyranoside
✍ Scribed by Cynthia B. Myers; Mercy M. Ramanjulu; H. L. Carrell; Jenny P. Glusker
- Book ID
- 105521104
- Publisher
- Springer
- Year
- 1997
- Tongue
- English
- Weight
- 500 KB
- Volume
- 8
- Category
- Article
- ISSN
- 1040-0400
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Sequential tritylation, benzoylation, and detritylation of methyl 3-deoxy-3fluoro-AD-galactop~~oside gave crystalline methyl 2,4-di-O-benzoyl-3-deoxy-3-~uoro-ED-gala~opyr~oside (9), which was used as the initial nucleophile in the synthesis of the target otigosaccha~de (16). Treatment of 9 with 2,3,