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Synthesis and x-ray crystal structure of 1,3,3-trinitroazetidine

✍ Scribed by Archibald, T. G.; Gilardi, Richard; Baum, K.; George, Clifford


Book ID
121403821
Publisher
American Chemical Society
Year
1990
Tongue
English
Weight
685 KB
Volume
55
Category
Article
ISSN
0022-3263

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Reaction of pentaerythrityl tetrabromide with fluorenyl potassium gave the title compound in 53% yield. The crystal structure revealed that in this unique trispiro[4.1.1.4.1.1]pentadecatetraene derivative, the adjacent rings are planar and orthogonal.