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Synthesis and structure of mononuclear molecular complexes of molybdenum(VI) and tungsten(VI) oxy- and dioxyhalides

✍ Scribed by V. L. Abramenko; V. S. Sergienko

Book ID
110182475
Publisher
SP MAIK Nauka/Interperiodica
Year
2009
Tongue
English
Weight
282 KB
Volume
54
Category
Article
ISSN
0036-0236

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## Abstract Reaction of WX~6~ (X = Cl or Br) with O(SiMe~3~)~2~ in CH~2~Cl~2~, followed by addition of MeCN and a further equivalent of O(SiMe~3~)~2~ in CH~2~Cl~2~ gives [WO~2~X~2~(MeCN)~2~] in situ, which subsequently react with the dithioethers MeS(CH~2~)~2~SMe, __i__PrS(CH~2~)~2~S__i__Pr or 1,4‐