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Synthesis and Structure of 8-Methyl-2-methylene-1,4,6,9-tetraoxaspiro[4.4]nonane

✍ Scribed by V. V. Zaitseva; T. G. Tyurina; S. Yu. Suikov; S. L. Bogza; S. P. Kobzev

Book ID
110349876
Publisher
SP MAIK Nauka/Interperiodica
Year
2002
Tongue
English
Weight
38 KB
Volume
38
Category
Article
ISSN
1070-4280

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## Abstract 8,9‐Benzo‐2‐methylene‐1,4,6‐trioxaspiro[4,4]nonane (BMTN) was prepared by the reaction of phthalide with epichlorohydrin, followed by dehydrochlorination. BMTN was polymerized with di‐__t__‐butyl peroxide (DTBP) to give a solyble polymer with a high molecular weight and good thermal sta