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Controlled free radical double ring-opening polymerization of 8,9-benzo-2-methylene-1,4,6-trioxaspiro[4,4]nonane

✍ Scribed by Xinru Jia; Mingqian Li; Shoufa Han; Ce Wang; Yen Wei

Book ID
117358162
Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
264 KB
Volume
31
Category
Article
ISSN
0167-577X

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Synthesis and polymerization of 8,9-benz
Synthesis and polymerization of 8,9-benzo-2-methylene-1,4,6-trioxaspiro[4,4]nonane (BMTN)
✍ Han, Yang Kyoo ;Choi, Sam Kwon πŸ“‚ Article πŸ“… 1983 πŸ› John Wiley and Sons βš– 466 KB

## Abstract 8,9‐Benzo‐2‐methylene‐1,4,6‐trioxaspiro[4,4]nonane (BMTN) was prepared by the reaction of phthalide with epichlorohydrin, followed by dehydrochlorination. BMTN was polymerized with di‐__t__‐butyl peroxide (DTBP) to give a solyble polymer with a high molecular weight and good thermal sta