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Synthesis and Photoinitiated Cationic Polymerization of 2-Methylene-7-phenyl-1,4,6,9-tetraoxaspiro[4.4]nonane

✍ Scribed by Bolln, Carsten; Frey, Holger; Mülhaupt, Rolf


Book ID
127334110
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
298 KB
Volume
29
Category
Article
ISSN
0024-9297

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Synthesis and polymerization of 8,9-benz
✍ Han, Yang Kyoo ;Choi, Sam Kwon 📂 Article 📅 1983 🏛 John Wiley and Sons ⚖ 466 KB

## Abstract 8,9‐Benzo‐2‐methylene‐1,4,6‐trioxaspiro[4,4]nonane (BMTN) was prepared by the reaction of phthalide with epichlorohydrin, followed by dehydrochlorination. BMTN was polymerized with di‐__t__‐butyl peroxide (DTBP) to give a solyble polymer with a high molecular weight and good thermal sta