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Synthesis and Structure of 1-Nitro-4-benzothiazolylsulfanyl- and -sulfonyldienes

✍ Scribed by T. Yu. Kretser; E. S. Lipina; G. A. Berkova; O. I. Evsyukova; N. V. Kuz'mina

Book ID
101989277
Publisher
John Wiley and Sons
Year
2006
Weight
20 KB
Volume
37
Category
Article
ISSN
0931-7597

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## Abstract 1‐(2‐Hydroxyethyl)‐2‐methyl‐5‐nitroimidazole (1) reacts with haloalkyltrialkylsilanes [Hal(CH~2~)~n~SiMe~2~R] to give 4‐nitroimidazole derivatives 3 and acetaldehyde. This process involves at least two reaction steps, __N__‐alkyl quaternization and elimination of the hydroxyethyl group.