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Synthesis and Structural Revision of Symbiodinolide C23−C34 Fragment

✍ Scribed by Murata, Takeshi; Sano, Masayuki; Takamura, Hiroyoshi; Kadota, Isao; Uemura, Daisuke

Book ID
123616694
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
873 KB
Volume
74
Category
Article
ISSN
0022-3263

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The degradation product C14ÀC23 2 was obtained using ethenolysis with the 2nd-generation Hoveyda-Grubbs catalyst from 62-membered lactone in symbiodinolide (1). The absolute configurations of three chiral centers in fragment 2 were assigned as 17R, 18R, and 21R by a combination of J-based configurat

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Symbiodinolide is a polyol macrolide isolated from the marine dinoflagellate Symbiodinium sp. in 2007. The C14-C24 fragment of symbiodinolide possessing the 17R/18R/21R absolute configuration, which was obtained as one of the degraded products of symbiodinolide, was synthesized stereoselectively fro