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Synthesis and spectroscopic characterisation of 3-chloroperbenzoic acid-17O,18O, nitrosobenzene-17O,18O and nitrosobenzene-15N

✍ Scribed by Christine Bleasdale; Martin K. Ellis; Peter B. Farmer; Bernard T. Golding; Kevin F. Handley; Peter Jones; William McFarlane

Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
362 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

3‐Chloroperbenzoic acid‐^17^O,^18^O was prepared from 3‐chlorobenzoyl chloride and hydrogen peroxide‐^17^O,^18^O (obtained by subjecting water‐^17^O,^18^O. Nitrobenzene‐^15^N was reduced to aniline‐^15^N, which was oxidised by 3‐chloroperbenzoic acid to nitrosobenzene‐^15^N. ^15^N and ^17^O NMR data are given for the corresponding labelled nitrosobenzene.

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