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Synthesis and spectral properties of 2,3-dihydro-2-[(o- and p-substituted)anilinylidene]-1H-4-(p-methylphenyl)-7-[(o- and p-methyl)phenoxy]-1,5-benzodiazepines

✍ Scribed by Eduardo Cortés Cortés; Maria Paz Sánchez Bravo

Publisher
Journal of Heterocyclic Chemistry
Year
1999
Tongue
English
Weight
367 KB
Volume
36
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

A series of twelve new 2,3‐dihydro‐2‐[(o‐ and p‐substituted)anilinylidene]‐1__H__‐4‐(p‐methylphenyl)‐7‐[(o‐ and p‐methyl)phenoxy]‐1,5‐benzodiazepines, which have potentially useful pharmacological properties, has been synthesized by condensing the 3,3‐dimercapto‐1‐(p‐methylphenyl)‐2‐propen‐1‐one with 3,4‐diaminophenyl‐R‐phenyl ethers. Subsequently the 1__H__‐1,5‐benzodiazepine‐2‐thiones obtained were treated with the (o‐ and p‐substituted)aniline. The structure of all products was corroborated by ir, ^1^H nmr, ^13^C nmr and ms.

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