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Synthesis and Redox Behavior of Azulene-Substituted Benzene Derivatives and (η 5 -Cyclopentadienyl)[tetra- and di(6-azulenyl)cyclobutadiene]cobalt Complexes

✍ Scribed by Ito, Shunji; Inabe, Haruki; Okujima, Tetsuo; Morita, Noboru; Watanabe, Masataka; Harada, Nobuyuki; Imafuku, Kimiaki

Book ID
126155071
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
197 KB
Volume
66
Category
Article
ISSN
0022-3263

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1,2-Di(6-azulenyl)tetraphenylbenzenes and (6-azulenyl)pentaphenylbenzenes were synthesized by Diels-Alder reaction of di(6-azulenyl)acetylenes and 6-(phenylethynyl)azulenes with tetraphenylcyclopentadienone. Mono(6-azulenyl)benzenes exhibited a reduction wave upon cyclic voltammetry (CV). In contras

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Synthesis and redox behavior of 1,3,5- a
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Described herein is a cobalt-mediated cyclooligomerization of mono-and di(6-azulenyl)acetylenes to afford 1,3,5-and 1,2,4-tri(6-azulenyl)benzene derivatives and (h 5 -cyclopentadienyl)[tetra-and di(6-azulenyl)cyclobutadiene]cobalt complexes. The redox behavior of these novel tri(6-azulenyl)benzene d