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Synthesis and Reactivity of Azepino[3,4-b]indol-5-yl Trifluoromethanesulfonate

✍ Scribed by Lidwine Chacun-Lefèvre; Benoı̂t Joseph; Jean-Yves Mérour

Book ID
108370847
Publisher
Elsevier Science
Year
2000
Tongue
French
Weight
178 KB
Volume
56
Category
Article
ISSN
0040-4020

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Preparation of the 5-substituted azepino [3,4-b]indole core structure can be realised through a catalytic Heck reaction. The scope and limitations of this methodology are reported. The reactivity of di-tert-butyl 5ethoxycarbonylmethylene-1,3,4,5-tetrahydro-1-oxoazepino[3,4-b]indole-2,10-dicarboxylat

Synthesis of 4-substituted azepino[3,4-b
Synthesis of 4-substituted azepino[3,4-b]indole-1,5-diones
✍ Julien Perron; Benoı̂t Joseph; Jean-Yves Mérour 📂 Article 📅 2003 🏛 Elsevier Science 🌐 French ⚖ 213 KB

Monoor dibromo derivatives 2 and 3 were prepared by an efficient two-step route from 10-methyl-azepino [3,4-b]indole-1,5dione 1. Elimination reaction on 2 gave access to 4-bromo-10-methyl-2H,10H-azepino[3,4-b]indole-1,5-diones 4. Finally, 4-substituted 10methyl-2H,10H-azepino [3,4-b]indole-1,5-dione