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Synthesis and Protein Binding of (4-Carboxybutyl)carbamoyl- Substituted Taxoids

✍ Scribed by Torsten Blitzke; Alexander Baranovsky; Bernd Schneider

Publisher: John Wiley and Sons
Year: 2001
Tongue: German
Weight: 91 KB
Volume: 84
Category: Article
ISSN: 0018-019X
DOI: 10.1002/1522-2675(20010711)84:7<1989::aid-hlca1989>3.0.co;2-m

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✦ Synopsis

4-Carboxybutyl)carbamates 5 and 6, as well as 10, derived from 10-O-deacetylbaccatin III (1) and paclitaxel (2), respectively, were synthesized by reaction of unprotected 1 and 2'-O-(methoxyacetyl)paclitaxel (8), respectively, with trimethylsilyl 5-isocyanatopentanoate in good yields. The carbamoyl-taxoids were conjugated to bovine-serum albumin and analyzed by MALDI-TOF mass spectrometry.

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