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Synthesis and molecular structure of the molybdate-bridged cyclic imido complex [Mo(S2CNEt2)2(NR) (μ-MoO4)]2 (R = 2,6-iPr2C6H3)

✍ Scribed by Thérèse A. Coffey; Glyn D. Forster; Graeme Hogarth

Book ID: 108328681
Publisher: Elsevier Science
Year: 1998
Tongue: English
Weight: 322 KB
Volume: 274
Category: Article
ISSN: 0020-1693
DOI: 10.1016/s0020-1693(97)06056-8

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## Abstract [LiN(SiMe~3~)Ar]~2~ (1, Ar = 2,6‐__i__Pr~2~C~6~H~3~) is prepared by the reaction of HN(SiMe~3~)Ar with __n__BuLi in __n__‐hexane. This compound with an unusual structure contains a four‐membered [LiN]~2~ heterocycle with two solvent‐free two‐coordinate Li centers. Its molecular structur