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Synthesis and Crystal Structure of the Nitrido Complexes [(n-Bu)4N]2 [{(L)Cl4ReN}2PtCl2] (L: THF, H2O) and [(n-Bu)4N]2 [(H2O)Cl4ReN-PtCl(μ-Cl)]2.

✍ Scribed by Simon Schwarz; Joachim Straehle

Publisher
John Wiley and Sons
Year
2010
Weight
40 KB
Volume
33
Category
Article
ISSN
0931-7597

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📜 SIMILAR VOLUMES

Synthese und Struktur der Nitrido-Komple
Synthese und Struktur der Nitrido-Komplexe [(n-Bu)4N]2[{(L)Cl4Re≡N}2PtCl2] (L = THF und H2O) und [(n-Bu)4N]2[(H2O)Cl4Re≡N-PtCl(μ-Cl)]2
✍ Simon Schwarz; Joachim Strähle 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 German ⚖ 105 KB 👁 1 views

Inhaltsübersicht. Der heteronukleare Dreikernkomplex [(n-Bu) 4 N] 2 [{(THF)Cl 4 ReϵN} 2 PtCl 2 ] (1a) entsteht bei der Reaktion von [(n-Bu) 4 N][ReNCl 4 ] mit [PtCl 2 (C 6 H 5 CN) 2 ] in THF/CH 2 Cl 2 in Form roter, solvathaltiger Kristalle. Er kristallisiert als 1a • 2 CH 2 Cl 2 in der tetragonalen

Synthesis and Crystal Structures of the
Synthesis and Crystal Structures of the Novel Tetrameric Nitrido Complexes [{cyclo-ReN}4(S2CNEt2)6(MeOH)2(PPh3)2][BPh4]2 · CH2Cl2 · 2 H2O and [{cyclo-ReN}4(S2CNEt2)4Cl4(PMe2Ph)4] · 2 acetone
✍ D. V. Griffiths; S. J. Parrott; M. Togrou; J. R. Dilworth; Yifan Zheng; S. Ritte 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 German ⚖ 141 KB 👁 2 views

Novel tetrameric rhenium(V) complexes have been prepared from [ReNCl 2 (PPh 3 ) 2 ] and [ReN(PMe 2 Ph) (S 2 CNEt) 2 ], respectively. [ReNCl 2 (PPh 3 ) 2 ] reacts with 1.5 equivalents of KS 2 CNEt 2 in methanol to yield the unusual dark red species [{cyclo-ReN} 4 (S 2 CNEt 2 . The crystal structure