Synthesis and Crystal Structure of Bis [1,2,3] Triazolo [1,5-a:4′,5′-d] Pyrimidin-9-Ones
✍ Scribed by Gerrit L'abbé; Françoise Godts; Suzanne Toppet; Luc Van Meervelt; Geoffrey S. D. King
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 2010
- Weight
- 267 KB
- Volume
- 96
- Category
- Article
- ISSN
- 0037-9646
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📜 SIMILAR VOLUMES
With sodium borohydride in tetrahydrofuran/ethanol (5 : 1). the product ( I ) gives a 75 yield of a compound, m.p. 233 "C, that is identical with the recently prepared 2-(diphenylmethyl)imidaz0le[~1. When product ( I ) is boiled for 2 h in tetrahydrofuran/water (2: I ) it affords 2-(hydroxy-dipheny
triphenylphosphanimino)tetrazolo [5,1-a][1,3,5]tri-An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14 N-NMR azine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural spectrum was