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Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine

✍ Scribed by Elmar Keßenich; Thomas M. Klapötke; Jörg Knizek; Heinrich Nöth; Axel Schulz

Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
193 KB
Volume
1998
Category
Article
ISSN
1434-1948

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✦ Synopsis

triphenylphosphanimino)tetrazolo [5,1-a][1,3,5]tri-An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14 N-NMR azine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts and crystal size. with the N4 atom of the triazine ring and forms a tetrazole.

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