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Synthesis, Characterization, and Crystal Structure of 1,3-Dipentafluorophenyl-2,2,2,4,4,4-hexazido-1,3-diaza-2,4-diphosphetidine

✍ Scribed by Christoph Aubauer; Konstatin Karaghiosoff; Thomas M. Klapötke; Gernot Kramer; Axel Schulz; Jan Weigand


Publisher
John Wiley and Sons
Year
2001
Tongue
German
Weight
139 KB
Volume
627
Category
Article
ISSN
0372-7874

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Crystal Structure of 4-(2-chlorophenyl)-
✍ D. Kumaran; M.N. Ponnuswamy; G. Jayanthi; V.T. Ramakrishnan; K. Panneerselvam; M 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 66 KB

The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Å, β = 104.49(2)º, V = 1539.2(7) Å 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ