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Synthesis and Crystal Structure of a New Mo(V) Complex of Cyano Ligands

✍ Scribed by Jie Qu; Wen Gu; Xin Liu

Book ID
106404265
Publisher
Springer
Year
2008
Tongue
English
Weight
414 KB
Volume
39
Category
Article
ISSN
1572-8854

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The reaction of 4-amino-6-methyl-1,2,4-triazine-3(2 H)-thione-5-one (AMTTO) with silver(I) nitrate in methanol gives the complex [Ag(AMTTO) 2 ]NO 3 (1). 1 was characterized by IR and 13 C NMR spectroscopy and by an X-ray structure analysis [space group C2/c, Z = 4, lattice dimensions at Β±80 Β°C: a =