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Synthesis and Characterization of Ph4Te4I4, Containing a Te4 Square, and Ph3PTe(Ph)I

✍ Scribed by Philip D. Boyle; Wendy I. Cross; Stephen M. Godfrey; Charles A. McAuliffe; Robin G. Pritchard; Shamsa Sarwar; Joanne M. Sheffield

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
156 KB
Volume
112
Category
Article
ISSN
0044-8249

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The synthesis of tetraphenylarsonium azi
The synthesis of tetraphenylarsonium azide, [Ph4As]+[N3]−, and the attempted preparation of tetraphenylarsonium azidodithiocarbonate, [Ph4As]+[SCSN3]−
✍ Margaret-Jane Crawford; Thomas M. Klapötke 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 142 KB 👁 2 views

Tetraphenylarsonium azide was prepared from the reaction of tetraphenylarsonium chloride monohydrate and sodium azide in aqueous solution. [Ph 4 As] ‫ם‬ [N 3 ] ‫מ‬ crystallizes in the orthorhombic space group P nma with Z ‫ס‬ 4 and unit cell dimensions a ‫ס‬ 16.539(2), b ‫ס‬ 10.879(2), and c ‫ס‬ 12.