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Synthesis and Molecular Structure of the Cu4P8 Cage Compound [Cu4(P4Ph4)2(PCyp3)3]

✍ Scribed by Robert Wolf; Evamarie Hey-Hawkins

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
110 KB
Volume
44
Category
Article
ISSN
0044-8249

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Blue crystals of metal nitratocuprates(II), M 3 [Cu(NO 3 ) 4 ](NO 3 ) (M = K (I), NH 4 (II), Rb (III)) and Cs 2 [Cu(NO 3 ) 4 ] (IV) were synthesized from Cu(NO 3 ) 2 3 H 2 O and MNO 3 by heating at 100±140 °C during 3±12 h. X-ray single crystal structures for isotypic I and II reveal the presence of