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Synthesis and Crystal Structure of [Ph4As]4[Au12S8], a Distorted Cubane-Like Thioaurate(I)

✍ Scribed by Dipl.-Chem. Gerolf Marbach; Prof. Dr. Joachim Strähle

Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
242 KB
Volume
23
Category
Article
ISSN
0044-8249

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The reactions of water-soluble phosphanes P(CH,OH), (1) and Ph2PCH20H (2) with NaAuC14 in aqueous or alcoholic media, produced the water/alcoholic-soluble Au' complexes [Au(P(CH,OH),),]+ (3) and [Au(Ph2PCH20H):J+ (4) in near quantitative yields. The X-ray structures of 3 and 4, reported in this pape