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Synthesis and characterization of organomolybdenum and organotungsten halides containing the η5-pentabenzylcyyclopentadienyl ligand η5-Bz5C5M(CO)3X (M  Mo, W; X  Cl, Br, I). The X-ray molecular structure of η5-Bz5C5Mo(CO)3I

✍ Scribed by Li-Cheng Song; Lu-Yan Zhang; Qing-Mei Hu; Xiao-Ying Huang

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
460 KB
Volume
230
Category
Article
ISSN
0020-1693

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Synthesis and Structure of the First η3-1,2-Diphosphaallyl Complexes [(η5-C5H5)(CO)2M{η3-RPPC(SiMe3)2}] (M = Mo, R = tBu, Cy; M = W, R = tBu) from [(η5-C5H5)(CO)2M=P=C(SiMe3)2] (M = Mo, W) and Inversely Polarized Phosphaalkenes RP=C(NMe2)2 (R = tBu, Cy)
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## Abstract Reaction of [(η^5^‐C~5~H~5~)(CO)~2~M=P=C(SiMe~3~)~2~] [where M = Mo (2), W (5)] with the phosphaalkene __t__BuP=C(NMe~2~)~2~ (1a) afforded the η^3^‐1,2‐diphosphaallyl complexes [(η^5^‐C~5~H~5~)(CO)~2~M{η^3^‐__t__BuPPC(SiMe~3~)~2~}], [where M = Mo (3a); M = W (6)]. Similarly, 2 and CyP=C