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Synthesis and Characterization of a Novel Dodecanuclear Porphyrin Ruthenium Cluster

โœ Scribed by Henrique E. Toma; Koiti Araki; Edegar O. Silva


Publisher
Springer Vienna
Year
1998
Tongue
English
Weight
194 KB
Volume
129
Category
Article
ISSN
0026-9247

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Novel biphasic synthesis of porphyrin
โœ Paul E. Ellis Jr; Wayne A. Langdale ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 28 KB

An unusual synthesis of porphyrin has been developed using a novel biphasic solvent system. Under optimized conditions reproducible yields of pure porphyrin of over 15% can be easily obtained in about two hours from the acid-catalysed condensation of 2-hydroxymethylpyrrole in a solvent consisting of