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Synthesis and biological activity of 25-hydroxy-2-methylene-vitamin D3 compounds

โœ Scribed by Sibilska, Izabela; Sicinski, Rafal R.; Plum, Lori A.; DeLuca, Hector F.


Book ID
121442362
Publisher
Elsevier Science
Year
2013
Tongue
English
Weight
612 KB
Volume
136
Category
Article
ISSN
0960-0760

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Synthesis of 25-hydroxy[26,27-3H]vitamin
โœ Joseph L. Napoli; Mary A. Fivizzani; Alan J. Hamstra; Heinrich K. Schnoes; Hecto ๐Ÿ“‚ Article ๐Ÿ“… 1979 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 556 KB

A synthesis of radiochemically pure 25-hydroxy[26,27-3H]vitamin D, with a specific activity of 160 Wmmol is reported. The structure and biological activity of the radiolabeled compound was verified by comigration on high-pressure liquid chromatography with synthetic 2Shydroxyvitamin D, to constant s