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Synthesis and addition reactions of aryl tetraethylphosphorodiamidites

✍ Scribed by N. A. Byina; I. A. Nuretdinov; N. P. Grechkin

Book ID: 112432297
Publisher: Springer
Year: 1967
Tongue: English
Weight: 247 KB
Volume: 16
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf00905371

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## Abstract Treatment of the sugar hemiacetals 1, 5, 7, 10, 12 and 14 with ArSSAr (Ar = phenyl, 2‐pyridyl, 2‐benzothiazolyl) and trialkylphosphanes affords in an S~N~2 process the corresponding aryl thioglycosides 3, 6, 8, 9, 11, 13, 15 and 16 in good to excellent yields. The reaction can be perfor