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Syntheses, spectra and crystal structures of ruthenium(II) complexes with polypyridyl: [Ru(bipy)2(phen)](ClO4)2 · H2O and [Ru(bipy)2(Me-phen)](ClO4)2

✍ Scribed by Bao-Hui Ye; Xiao-Ming Chen; Tian-Xian Zeng; Liang-Nian Ji

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
595 KB
Volume
240
Category
Article
ISSN
0020-1693

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✍ Mathias S. Wickleder 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 181 KB 👁 2 views

Single crystals of Lu(ClO 4 ) 3 ´3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 ´6 H 2 O at 140 °C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)°, b = 79.18(2), c = 63.83(2), R all = 0.