Single crystals of Lu(ClO 4 ) 3 ´3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 ´6 H 2 O at 140 °C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)°, b = 79.18(2), c = 63.83(2), R all = 0.
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ChemInform Abstract: Perchlorato Complexes of Rare-Earth Elements: Syntheses and Crystal Structures of Lu(ClO4)3×3H2O, Er(ClO4)3×H2O, and Sc(OH)(ClO4)2×H2O.
✍ Scribed by Mathias S. Wickleder
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 34 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0931-7597
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