Single crystals of Lu(ClO 4 ) 3 ´3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 ´6 H 2 O at 140 °C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)°, b = 79.18(2), c = 63.83(2), R all = 0.
Hydroxo Bridged Dinuclear Rare Earth Complexes: Syntheses and Crystal Structures of [Ln2(phen)4(H2O)4(OH)2](NO3)4(phen)2 with Ln = Er, Lu
✍ Scribed by Yue-Qing Zheng; Lin-Xia Zhou; Jian-Li Lin; Sun-Wei Zhang
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- German
- Weight
- 122 KB
- Volume
- 627
- Category
- Article
- ISSN
- 0372-7874
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