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Syntheses, crystal structures and spectroscopic properties of Ag2Nb[P2S6][S2] and KAg2[PS4]

✍ Scribed by Yuandong Wu; Wolfgang Bensch

Book ID
104030285
Publisher
Elsevier Science
Year
2009
Tongue
English
Weight
589 KB
Volume
182
Category
Article
ISSN
0022-4596

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Bis(disulfido) bridged Nb IV cluster oxalate complexes [Nb 2 (S 2 ) 2 (C 2 O 4 ) 4 ] 4Β± were prepared by ligand substitution reaction from the aqua ion [Nb 2 (l-S 2 ) 2 (H 2 O) 8 ] 4+ and isolated as K 4 (3). The crystal structures of 1 and 2 were determined. The crystals of 1 belong to the space