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Structure of naphtho[1,8-de][1,2]oxathiepin 3-oxide

✍ Scribed by Olivier, M. J. ;Brisse, F. ;Harpp, D. N. ;Steliou, K.

Book ID
114504114
Publisher
International Union of Crystallography
Year
1988
Tongue
English
Weight
439 KB
Volume
44
Category
Article
ISSN
0108-2701

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The photolysis of naphtho[1,8-de]-l,3-dichalcogeninylidene 1-oxide derivatives (4 and 5) at >290 nm generates ketenes together with naphtho[1,8-cd]-l,2-dichalcogenole, which were confirmed by the trapping experiments and the direct observation using IR spectroscopy. The generation of ketenes from th