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Structure of Dibenzocrown Ethers and their H-Bonded Adducts.1. [1.5]Dibenzo-18-Crown-6 and Biphenyl-20-Crown-6: Complexes with Amidosulfuric Acid

✍ Scribed by Sergei A. Kotlyar; Marina S. Fonari; Yurii A. Simonov; Gabriele Bocelli; Oleg V. Shishkin; Svetlana V. Shishkina; Vyacheslav V. Tkachuk; Ruslan Ya. Grygorash; Gerbert L. Kamalov


Publisher
Springer Netherlands
Year
2005
Tongue
English
Weight
726 KB
Volume
52
Category
Article
ISSN
0923-0750

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For both structures all hydrogens were located in difference Fourier syntheses. The structures were refined by least-squares methods (OWLS ' ' 1 ; scale factor, isotropic extinction parameter, position parameters, anisotropic thermal parameters for non-Hatoms, isotropic thermal parameters for H) to