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Structure elucidation of an unexpected product from dehydration of a β-hydroxyketone

✍ Scribed by David E. Minter; Christopher D. Winslow; William H. Watson; Satish Bodige

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
162 KB
Volume
44
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The structure of an unexpected compound from the dehydration of an aldol addition product has been determined using 1‐D and 2‐D NMR techniques. This reaction is the last step in a new synthetic approach to the galanthan ring system. Complete ^1^H and ^13^C NMR assignments for two synthetic precursors are also reported. Copyright © 2006 John Wiley & Sons, Ltd.

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