𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Structure elucidation of an unexpected acylation product of dithranol: An application of improved heteronuclear two-dimensional NOE spectroscopy

✍ Scribed by P. Bigler; M. Rychener; U. Séquin

Publisher
John Wiley and Sons
Year
1988
Tongue
English
Weight
385 KB
Volume
26
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Assignment of Quaternary Carbon Atoms in
Assignment of Quaternary Carbon Atoms in 13C-NMR Spectroscopy: Application of an improved heteronuclear 2D-NOE experiment
✍ Peter Bigler 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 German ⚖ 286 KB

Nuclear Overhauser effects (NOE) between protons and heteronuclei can be of great value for the assignment of quaternary nuclei, and they can be very informative and unique in view of stereochemistry and molecular dynamics. The application of a modified 2D-NMR experiment for the assignment of quater

Automated structure elucidation of two u
Automated structure elucidation of two unexpected products in a reaction of an α,β-unsaturated pyruvate
✍ Gary J. Sharman; Ian C. Jones; Mark P. Parnell; Michael C. Willis; Mary F. Mahon 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 115 KB

## Abstract The reaction between an α,β‐unsaturated pyruvate and ethyl diazoacetate (EDA) yielded two unexpected products. The structures of these products were determined by automated elucidation of the chemical structures using spectroscopic inputs of a series of 1D and 2D NMR data using the comp

Derivatization reaction of the mycotoxin
Derivatization reaction of the mycotoxin moniliformin with 1,2-diamino-4,5-dichlorobenzene: structure elucidation of an unexpected reaction product by liquid chromatography/tandem mass spectrometry and liquid chromatography/nuclear magnetic resonance spectroscopy
✍ Peter Zöllner; Annette Lienau; Klaus Albert; Wolfgang Lindner 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 125 KB

## Abstract The derivatization reaction of the mycotoxin moniliformin with 1,2‐diamino‐4,5‐dichlorobenzene was previously introduced to improve distinctly the sensitivity of an assay applying high‐performance liquid chromatography prior to fluorescence detection. In the course of the implementation