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Structure elucidation and 1H/13C NMR spectral assignments of four trabectedin related compounds

✍ Scribed by Wim Vermeulen; Walter Filliers; Carmen García; Sonia Manzanaro; David Montalvo; Concepción Polanco; Frank Spillemaeckers; Bart Van Hoof; Guido Winderickx; Ivan Somers; Ignacio Rodriguez-Campos

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
120 KB
Volume
46
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

This article presents the structure elucidation of four new compounds, formed during the hemisynthetic preparation of trabectedin, an anti‐tumor natural product from Ecteinascidia turbinata. We report herein on the use of UV, MS and NMR spectroscopic data along with ^1^H and ^13^C spectral assignments obtained by means of 1D and 2D homo‐ and heteronuclear NMR techniques. Copyright © 2008 John Wiley & Sons, Ltd.

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