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Structural study of molybdenum(VI) complexes containing bidentate ligands: Synthesis, characterization and DFT calculations

✍ Scribed by Raúl Colorado-Peralta; Mario Sanchez-Vazquez; Irán F. Hernández-Ahuactzi; Sonia A. Sánchez-Ruiz; Rosalinda Contreras; Angelina Flores-Parra; Silvia E. Castillo-Blum

Book ID
118163646
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
990 KB
Volume
48
Category
Article
ISSN
0277-5387

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## Abstract Reaction of WX~6~ (X = Cl or Br) with O(SiMe~3~)~2~ in CH~2~Cl~2~, followed by addition of MeCN and a further equivalent of O(SiMe~3~)~2~ in CH~2~Cl~2~ gives [WO~2~X~2~(MeCN)~2~] in situ, which subsequently react with the dithioethers MeS(CH~2~)~2~SMe, __i__PrS(CH~2~)~2~S__i__Pr or 1,4‐