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Stereospecific total synthesis of aphidicolin

✍ Scribed by McMurry, John E.; Andrus, Alex; Ksander, Gary M.; Musser, John H.; Johnson, Mark A.

Book ID
126289348
Publisher
American Chemical Society
Year
1979
Tongue
English
Weight
379 KB
Volume
101
Category
Article
ISSN
0002-7863

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A Total Synthesis of Aphidicolin: Stereo
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## Abstract A simple, efficient, and stereospecific total synthesis of (Β±)‐3Ξ±, 18‐dihydroxy‐17‐noraphidicolan‐16‐one **(2)**, by solvolytic rearrangement of the __endo__‐bicyclo‐[2.2.2]oct‐5‐en‐2‐yl methanesulfonate **16**, is described. Since aphidicolin **(1)** has already been obtained from **2*

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