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Spectral assignment of 2″-O-β-D-glucopyranosylsaikosaponin b2 by two-dimensional NMR techniques

✍ Scribed by Long-Ze Lin; Lee-Juian Lin; Geoffrey A. Cordell; Si-Qi Luo; Hui-Fang Jiang

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
657 KB
Volume
30
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

A new derivative of saikosaponin was isolated from the roots of Bupleurum longicaule and identified as 2″‐O‐β″‐D‐glucopyranosylsaikosaponin b2. Its ^1^H and ^13^C NMR data and the connectivities of the sugar moiety were assigned by use of a combination of two‐dimensional NMR techniques (DQF‐COSY, HOHAHA, ROESY, HETCOR and HMBC).

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