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Some technical improvements in the paper chromatography of keto acid 2,4-dinitrophenylhydrazones

✍ Scribed by A.S. Saini


Publisher
Elsevier Science
Year
1967
Tongue
English
Weight
292 KB
Volume
26
Category
Article
ISSN
1873-3778

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Thin-layer chromatography of keto acid 2
✍ Nakao Ariga πŸ“‚ Article πŸ“… 1972 πŸ› Elsevier Science 🌐 English βš– 334 KB

Thin-layer chromatography of keto acid 2,4-dinitrophenylhydrazones was carried out on plate coated with silica gel and sodium bicarbonate. A clear separation was obtained between most of the various keto acid hydrazones. The hydrazone was eluted from the plate with methanol containing 1% concentrate

Improved method for the separation and c
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For characterizing keto acids, paper chromatography of their DNPHa is most widely used irrespective of the disadvantages (1)) some of which are as follows: According to the methods reported before 1962, the DNPH formed by the usual method were extracted from water solution with an organic solvent su