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Solvent-Free Cycloaddition Reaction of 3-Indolylimines with Chloroacetyl Chloride under Microwave Irradiation.

✍ Scribed by Anshu Dandia; Ruby Singh; Pragati Sharma

Publisher
John Wiley and Sons
Year
2003
Weight
105 KB
Volume
34
Category
Article
ISSN
0931-7597

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πŸ“œ SIMILAR VOLUMES

Solvent-free cycloaddition reaction of 3
Solvent-free cycloaddition reaction of 3-indolylimines with chloroacetyl chloride under microwave irradiation
✍ Anshu Dandia; Ruby Singh; Pragati Sharma πŸ“‚ Article πŸ“… 2003 πŸ› John Wiley and Sons 🌐 English βš– 114 KB πŸ‘ 1 views

## Abstract Solvent‐free approach is developed for the rapid synthesis of spiro[azetidine‐indoles] **__6a–g__** on basic alumina supported potassium carbonate (K~2~CO~3~–Al~2~O~3~) from the cycloaddition reaction of indolylimines **__3__** and chloroacetyl chloride **__4__** as synthons using micro

Synthesis of oximes, conversion to nitri
Synthesis of oximes, conversion to nitrile oxides and their subsequent 1,3-dipolar cycloaddition reactions under microwave irradiation and solvent-free reaction conditions
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Aldoximes and ketoximes were readily synthesized from aldehydes and hydroxylamine hydrochloride on Al 2 O 3 without solvent under microwave irradiation. At higher irradiation power, aldoximes dehydrated to nitriles and ketoximes rearranged to amides. Aldoximes reacted in a one-pot reaction with Nchl