Solution Synthesis and Characterization of Aza-β 3 -peptides (N α -Substituted Hydrazino Acetic Acid Oligomers)
✍ Scribed by Cheguillaume, Arnaud; Salaün, Arnaud; Sinbandhit, Sourisak; Potel, Michel; Gall, Philippe; Baudy-Floc'h, Michèle; Le Grel, Philippe
- Book ID
- 126989859
- Publisher
- American Chemical Society
- Year
- 2001
- Tongue
- English
- Weight
- 114 KB
- Volume
- 66
- Category
- Article
- ISSN
- 0022-3263
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📜 SIMILAR VOLUMES
Two new glycosyl amino acids N'~-Fmoc-Ser[Ac4-fl-D-Galp-(1 ~ 3)-Ac2-a-D-GalN3P]-OPf p and N'~-Fmoc-Thr[Ac4-/3-D-Galp-(1 ~ 3)-Ac2-a-D-GalN3p]-OPf p were synthesized. Glycosylation of N'~-Fmoc-Ser-OPf p or N ~-Fmoc-Thr-OPfp with protected/3-o-Gal-( 1 -~ 3)-D-GaIN 3 donors afforded the glycosyl amino a
The dehydro-residue containing peptides N-Ac-dehydro-Phe-L-Leu-OCH3 ( I ) and N-Acdehydro-Phe-NorVal-OCH, (11) were synthesized by the usual workup procedures. The peptides crystallize from their solutions in methanol in space group P6,: ( I ) a = b = 12.528(2) A, c = 21.653(5) A; (11) a = b = 12.53