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Solid-Phase Synthesis of 4,6-Disubstituted and 3,4,6-Trisubstituted Pyrid-2-ones

โœ Scribed by Katritzky, Alan R.; Chassaing, Christophe; Barrow, Stuart J.; Zhang, Zenghong; Vvedensky, Vladimir; Forood, Behrouz

Book ID
111925918
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
35 KB
Volume
4
Category
Article
ISSN
1520-4766

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Solid phase synthesis of 2,4,5-trisubsti
Solid phase synthesis of 2,4,5-trisubstituted thiomorpholin-3-ones
โœ Adel Nefzi; Marc Giulianotti; Richard A. Houghten ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 170 KB

The solid phase synthesis of 2,4,5-trisubstituted thiomorpholin-3-ones is described. Starting from a resin-bound protected cysteine, and employing reductive alkylation and amide formation, thiomoq~holin-3one derivatives have been synthesized through intramolecular thioether formation in good yield a