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Solid-Phase Synthesis of 3,4,5-Substituted 1,5-Benzodiazepin-2-ones †

✍ Scribed by Lee, Jung; Gauthier, Diane; Rivero, Ralph A.

Book ID
127212974
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
87 KB
Volume
64
Category
Article
ISSN
0022-3263

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Solid-phase synthesis of 1,5-benzodiazep
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A solid-phase synthesis ofpolysubstituted 1,5-benzodiazepin-2-ones is described. Resinbound 4-fluoro-3-nitrobanzoic acid was reacted with different ~amino acids, followed by nitro group reduction and formation of the seven-membered ring. Subsequent alkylations at N(5) and N(1) afforded the title com

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