Simultaneous analysis of hydrocortisone
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J. Korpi; D. P. Wittmer; B. J. Sandmann; W. G. Haney Jr.
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Article
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1976
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John Wiley and Sons
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English
β 300 KB
Compounds IVb-IVg were prepared similarly from I11 and the appropriate alcohols (Table I). p-Chlorophenyl Benzo[ b]-3-methyl-2-furancarbamate (1Vb)-A solution of I11 (2.01 g, 0.01 mole) and p-chlorophenol(l.28 g, 0.01 mole) in 30 ml of dry benzene was refluxed for 4 hr. The solvent was evaporated,