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Silicon-Nitrogen Heterocycles containing CN Double Bonds

✍ Scribed by Dr. O. J. Scherer; Dipl.-Chem. P. Hornig


Publisher
John Wiley and Sons
Year
1967
Tongue
English
Weight
127 KB
Volume
6
Category
Article
ISSN
0044-8249

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Compound ( I ) is heated with 1.5 mol. equiv. of hydroquinone and 2.5 mol. equiv. of potassium tert-butoxide in water (corresponding to 0.5 N KOH) under Nz for three weeks in a sealed tube at 110°C. Acidification of the reaction mixture, filtration, and washing of the filter cake neutral with water,