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Scalable Synthesis of Enantiomerically Pure Bicyclo[2.2.2]octadiene Ligands

โœ Scribed by Abele, Stefan; Inauen, Roman; Spielvogel, Dirk; Moessner, Christian

Book ID
127122120
Publisher
American Chemical Society
Year
2012
Tongue
English
Weight
544 KB
Volume
77
Category
Article
ISSN
0022-3263

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## Abstract The addition of difluorocarbene to bicyclo[2.2.2]octaโ€2,5โ€diene gave the __exo__ and __endo__ 1:1 cyclopropane adducts. In contrast to norbornadiene, no __homo__โ€1,4 adduct was formed. The adducts were thermally stable under the conditions of their formation and separation (<170ยฐ). Howe