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(R,R)-4,4′-Dimethyl-2,2′-[cyclo­hexane-1,2-diylbis(nitrilomethylidyne)]diphenol

✍ Scribed by Yang, Ming-Hua ;Zheng, Yun-Fa ;Yan, Guo-Bing

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
124 KB
Volume
63
Category
Article
ISSN
1600-5368

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(1R,2R)-(+)-4,4′-Di-tert-butyl-2,2′-[1,2
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The crystal structure of the title compound, C~36~H~40~N~2~O~2~, has been determined at 173 (2) K. The molecule has __C__ ~2~ symmetry and the asymmetric unit contains one half-molecule. An intramolecular O—H...N hydrogen bond is formed between the phenol OH group and the Schiff base N atom.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.053 wR factor = 0.143 Data-to-parameter ratio = 14.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

The cocrystal {4,4′-dimethoxy-2,2′-[prop
The cocrystal {4,4′-dimethoxy-2,2′-[propane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol(pyridine)manganese(III) hexafluoridophosphate–{4,4′-dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol(pyridine)manganese(III) hexafluoridophosphate (1/1)
✍ Habibi, Mohammad Hossein ;Askari, Elham ;Chantrapromma, Suchada ;Fun, Hoong-Kun 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 746 KB

The cocrystal {4,4 0 0 0 -dimethoxy-2,2 0 0 0 -[propane-1,2-diylbis(nitrilomethylidyne)]-diphenolato}methanol(pyridine)manganese(III) hexafluoridophosphate-{4,4 0 0 0dimethoxy-2,2 0 0 0 -[ethane-1,2-diylbis-(nitrilomethylidyne)]diphenolato}methanol(pyridine)manganese(III) hexafluoridophosphate (1/1