𝔖 Bobbio Scriptorium
✦   LIBER   ✦

(1R,2R)-(+)-4,4′-Di-tert-butyl-2,2′-[1,2-diphenyl­ethane-1,2-diylbis(nitrilo­methyl­idyne)]diphenol

✍ Scribed by Korendovych, Ivan V. ;Makhlynets, Olga V. ;Buzak, Sara K. ;Flook, Margaret M. ;Kryatov, Sergey V. ;Haas, Terry E. ;Rybak-Akimova, Elena V.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
281 KB
Volume
62
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

The crystal structure of the title compound, C~36~H~40~N~2~O~2~, has been determined at 173 (2) K. The molecule has C
~2~ symmetry and the asymmetric unit contains one half-molecule. An intramolecular O—H...N hydrogen bond is formed between the phenol OH group and the Schiff base N atom.

📜 SIMILAR VOLUMES

{2,2′-[Ethane-1,2-diylbis(nitrilo­methyl
{2,2′-[Ethane-1,2-diylbis(nitrilo­methyl­idyne)]diphenoxy­acetato}zinc(II) methanol solvate
✍ Wang, Jing ;Zhu, Dong-Sheng ;Shao, Kui-Zhan ;Xu, Lin 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 204 KB

The title compound, [Zn(C 20 H 18 N 2 O 6 )]ÁCH 3 OH, has been synthesized through a one-step procedure in a methanol solvent. The Zn atom exhibits a distorted trigonal prismatic geometry consisting of two imine N-atom donors, two O-atom donors of the phenoxy groups and two O-atom donors of the depr

{6,6′-Dimeth­oxy-2,2′-[ethane-1,2-diylbi
{6,6′-Dimeth­oxy-2,2′-[ethane-1,2-diylbis(nitrilo­methyl­idyne)]diphenolato}(ethanol)dioxouranium(VI)
✍ Şenyüz, Nuray ;Yüksektepe, Çiĝdem ;Batı, Hümeyra ;Çalışkan, Nezihe ;Büyükgüngör, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 250 KB

{6,6 0 0 0 -Dimethoxy-2,2 0 0 0 -[ethane-1,2-diylbis-(nitrilomethylidyne)]diphenolato}(ethanol)dioxouranium(VI) Nuray S ¸enyu ¨z, a C ¸ig ˆdem Yu ¨ksektepe, b \* Hu ¨meyra Batı, a Nezihe C ¸alıs ¸kan b and Orhan Bu ¨yu ¨kgu ¨ngo ¨rb

2,2′-{(Z)-Ethane-1,2-diyl­bis­[(Z)-o-phe
2,2′-{(Z)-Ethane-1,2-diyl­bis­[(Z)-o-phenyl­ene­nitrilo­methyl­idyne]}diphenol (EIEP)
✍ Sony, S. M. Malathy ;Charles, P. ;Ponnuswamy, M. N. ;Yathirajan, H. S. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 282 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.057 wR factor = 0.199 Data-to-parameter ratio = 21.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.